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药物分析中的分离技术

作者: 唐安娜著 , 董襄朝著

出版社: 南开大学出版社

出版时间: 2022-11

版次: 1

ISBN: 9787310063345

装帧: 平装

开本: 16开

纸张: 胶版纸

页数: 158页

字数: 269.000千字

正文语种: 简体中文，英语

分类: 医药卫生

1人买过

  This textbook is for undergraduate and graduate students who are in chemistry major and English as a second language. It is developed from the teaching material of the class： Separation Technology in the Pharmaceutical Analysis. This textbook is aimed to provide better teaching material for the students who take the class in the College of Chemistry， Nankai University and major in related disciplines.
  Separation is an important part of chemical analysis. This textbook introduces the knowledge of separation technology and its application in pharmaceutical analysis. Opening of all English courses in chemistry benefits the improvement of students in both major profession and professional English.
  In 2004， Professor Xiangchao Dong opened the full English class of \"separation technology in the pharmaceutical analysis\" for undergraduate and graduate students in College of Chemistry， Nankai University. It is a one semester optional course with 2 hour lecture each week. The teaching material was independently compiled by Prof. Xiangchao Dong. After about 12 years of class practice and continuous improvement， a relatively complete teaching material including chromatography and capillary electrophoresis as major parts has been formed. Dr. Anna Tang continues to teach the class after 2017 and brings new teaching ideas. Dr. Anna Tang also adds new teaching contents of separation technologies in biochemical drug， non-targeted screening analysis and new material development for pharmaceutical separations. In order to make a better understanding， Dr. Anna Tang adds questions and problems for students to study. She is also involved in the proofreading in all of the contents. 唐安娜，南开大学化学学院副教授，硕士生导师。2004.7毕业于南开大学化学学院分析化学专业，获理学博士学位并留校任教。2010.9-2011.9在美国亚利桑那大学化学与生物系做访问学者。讲授本科生《仪器分析》课程；讲授本科生、研究生《药物分析中的分离技术》课程。获校级全英文课程建设项目一项、教材建设项目一项，化学学院教材建设项目一项。已有多篇教改论文在《大学化学》《化学教育》上发表。 CHAPTER 1 INTRODUCTION TO THE PHARMACEUTIC ALANALYSIS
1．1 Nature and Tasks of Pharmaceutical Analysis
1．1．1 Pharmaceutical Analysis in the New Drug Discovery
1．1．2 Pharmaceutical Analysis to Ensure the Quality of Drug Product
1．1．3 Pharmaceutical Analysis in the Stability Studies
1．1．4 In Vivo Drug Analysis
1．2 National Standards for Supervision of Drug Quality
1．3 Significance of Separation Technology in the Pharmaceutical Analysis

CHAPTER 2 CHROMATOGRAPHIC ANALYSIS
2．1 Theoretical Principle and Parameters
2．1．1 Theoretical Principles
2．1．2 Separation Parameters
2．1．3 Theoretical Plates of a Chromatographic Column
2．2 Gas Chromatography
2．2．1 Separation Mechanism
2．2．2 GC Instrument
2．2．3 GC Columns
2．2．4 Stationary Phases in GC
2．2．5 Stationary Phases in the GSC
2．2．6 Stationary Phases in the GLC
2．2．7 Detectors in GC
2．2．8 Advantages of GC
2．2．9 Applications of GC
2．3 Introduction to Liquid Chromatography
2．3．1 Columns in HPLC
2．3．2 General Morphology of HPLC Stationary Phase Particles
2．4 Normal Phase Liquid Chromatography
2．4．1 Characteristics of Normal Phase Liquid Chromatography
2．4．2 Elution Ability of Mobile Phase
2．4．3 Applications
2．5 Reversed-phase Liquid Chromatography
2．5．1 Stationary Materials for Reversed-phase Liquid Chromatography
2．5．2 Retention Characteristic of Reversed-phase Chromatography
2．5．3 Secondary Chemical Equilibria in the Reversed-phase Chromatography
2．5．4 Applications of Reversed-phase HPLC
2．5．5 Ion-pair Reversed-phase Chromatography
2．6 Ion-exchange Chromatography
2．6．1 Separation Principle of IEC
2．6．2 Stationary Phase Materials of IEC
2．6．3 Retention of Analyses in IEC
2．6．4 Major Factors in the IEC Separation
2．6．5 Detection in IEC
2．6．6 Advantages of IEC
2．6．7 Application
2．7 Size-exclusion Chromatography
2．7．1 Separation Mechanism
2．7．2 Packing Materials for SEC
2．7．3 Applications of SEC
2．8 Affinity Chromatography
2．8．1 Nature of Affinity Interaction
2．8．2 Separation Principle of Affinity Chromatography
2．8．3 Ligand Selection
2．8．4 Selection of Supporting Materials
2．8．5 Preparation of Packing Materials for Affinity Chromatography
2．8．6 Separation by Affinity Chromatography
2．8．7 Application of Affinity Separation Technology
2．9 Thin-layer Chromatography
2．9．1 Stationary Phases Used in TLC
2．9．2 Operation in TLC
2．9．3 Performance Characteristics of TLC
2．9．4 Detection in TLC
2．9．5 Quantitative Analysis
2．9．6 Applications of TLC Analysis
2．10 Detectors in Liquid Chromatography
2．10．1 Bulk Property Detectors
2．10．2 Solute Property Detectors
References
……

CHAPTER 3 HIGH PERFORMANCE CAPILLARY ELECTROPHORESIS AND ITSAPPLICATIONIN PHARMACEUTICAL ANALYSIS
CHAPTER 4 APPLICATION OF SEPARATION TECHNOLOGYIN BIOCHEMICAL DRUG ANALYSIS AND DISEASE DIAGNOSIS
CHAPTER 5 NON-TARGETED SCREENING IN THE ANALYSIS OF COMPLEX SAMPLES WITH UNKNOWN COMPONENTS
CHAPTER 6 NEW MATERIAL DEVELOPMENT FOR PHARMACEUTICALSEPARATIONS

QUESTIONS AND PROBLEMS

INDEX
内容简介:
  This textbook is for undergraduate and graduate students who are in chemistry major and English as a second language. It is developed from the teaching material of the class： Separation Technology in the Pharmaceutical Analysis. This textbook is aimed to provide better teaching material for the students who take the class in the College of Chemistry， Nankai University and major in related disciplines.
  Separation is an important part of chemical analysis. This textbook introduces the knowledge of separation technology and its application in pharmaceutical analysis. Opening of all English courses in chemistry benefits the improvement of students in both major profession and professional English.
  In 2004， Professor Xiangchao Dong opened the full English class of \"separation technology in the pharmaceutical analysis\" for undergraduate and graduate students in College of Chemistry， Nankai University. It is a one semester optional course with 2 hour lecture each week. The teaching material was independently compiled by Prof. Xiangchao Dong. After about 12 years of class practice and continuous improvement， a relatively complete teaching material including chromatography and capillary electrophoresis as major parts has been formed. Dr. Anna Tang continues to teach the class after 2017 and brings new teaching ideas. Dr. Anna Tang also adds new teaching contents of separation technologies in biochemical drug， non-targeted screening analysis and new material development for pharmaceutical separations. In order to make a better understanding， Dr. Anna Tang adds questions and problems for students to study. She is also involved in the proofreading in all of the contents.
作者简介:
唐安娜，南开大学化学学院副教授，硕士生导师。2004.7毕业于南开大学化学学院分析化学专业，获理学博士学位并留校任教。2010.9-2011.9在美国亚利桑那大学化学与生物系做访问学者。讲授本科生《仪器分析》课程；讲授本科生、研究生《药物分析中的分离技术》课程。获校级全英文课程建设项目一项、教材建设项目一项，化学学院教材建设项目一项。已有多篇教改论文在《大学化学》《化学教育》上发表。
目录:
CHAPTER 1 INTRODUCTION TO THE PHARMACEUTIC ALANALYSIS
1．1 Nature and Tasks of Pharmaceutical Analysis
1．1．1 Pharmaceutical Analysis in the New Drug Discovery
1．1．2 Pharmaceutical Analysis to Ensure the Quality of Drug Product
1．1．3 Pharmaceutical Analysis in the Stability Studies
1．1．4 In Vivo Drug Analysis
1．2 National Standards for Supervision of Drug Quality
1．3 Significance of Separation Technology in the Pharmaceutical Analysis

CHAPTER 2 CHROMATOGRAPHIC ANALYSIS
2．1 Theoretical Principle and Parameters
2．1．1 Theoretical Principles
2．1．2 Separation Parameters
2．1．3 Theoretical Plates of a Chromatographic Column
2．2 Gas Chromatography
2．2．1 Separation Mechanism
2．2．2 GC Instrument
2．2．3 GC Columns
2．2．4 Stationary Phases in GC
2．2．5 Stationary Phases in the GSC
2．2．6 Stationary Phases in the GLC
2．2．7 Detectors in GC
2．2．8 Advantages of GC
2．2．9 Applications of GC
2．3 Introduction to Liquid Chromatography
2．3．1 Columns in HPLC
2．3．2 General Morphology of HPLC Stationary Phase Particles
2．4 Normal Phase Liquid Chromatography
2．4．1 Characteristics of Normal Phase Liquid Chromatography
2．4．2 Elution Ability of Mobile Phase
2．4．3 Applications
2．5 Reversed-phase Liquid Chromatography
2．5．1 Stationary Materials for Reversed-phase Liquid Chromatography
2．5．2 Retention Characteristic of Reversed-phase Chromatography
2．5．3 Secondary Chemical Equilibria in the Reversed-phase Chromatography
2．5．4 Applications of Reversed-phase HPLC
2．5．5 Ion-pair Reversed-phase Chromatography
2．6 Ion-exchange Chromatography
2．6．1 Separation Principle of IEC
2．6．2 Stationary Phase Materials of IEC
2．6．3 Retention of Analyses in IEC
2．6．4 Major Factors in the IEC Separation
2．6．5 Detection in IEC
2．6．6 Advantages of IEC
2．6．7 Application
2．7 Size-exclusion Chromatography
2．7．1 Separation Mechanism
2．7．2 Packing Materials for SEC
2．7．3 Applications of SEC
2．8 Affinity Chromatography
2．8．1 Nature of Affinity Interaction
2．8．2 Separation Principle of Affinity Chromatography
2．8．3 Ligand Selection
2．8．4 Selection of Supporting Materials
2．8．5 Preparation of Packing Materials for Affinity Chromatography
2．8．6 Separation by Affinity Chromatography
2．8．7 Application of Affinity Separation Technology
2．9 Thin-layer Chromatography
2．9．1 Stationary Phases Used in TLC
2．9．2 Operation in TLC
2．9．3 Performance Characteristics of TLC
2．9．4 Detection in TLC
2．9．5 Quantitative Analysis
2．9．6 Applications of TLC Analysis
2．10 Detectors in Liquid Chromatography
2．10．1 Bulk Property Detectors
2．10．2 Solute Property Detectors
References
……

CHAPTER 3 HIGH PERFORMANCE CAPILLARY ELECTROPHORESIS AND ITSAPPLICATIONIN PHARMACEUTICAL ANALYSIS
CHAPTER 4 APPLICATION OF SEPARATION TECHNOLOGYIN BIOCHEMICAL DRUG ANALYSIS AND DISEASE DIAGNOSIS
CHAPTER 5 NON-TARGETED SCREENING IN THE ANALYSIS OF COMPLEX SAMPLES WITH UNKNOWN COMPONENTS
CHAPTER 6 NEW MATERIAL DEVELOPMENT FOR PHARMACEUTICALSEPARATIONS

QUESTIONS AND PROBLEMS

INDEX

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药物分析中的分离技术

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