北五味子化学成分分析及利用（英文版）

作者: 马春慧著 , 杨磊著 , 祖元刚著

出版社: 科学出版社

出版时间: 2014-06

版次: 1

ISBN: 9787030406071

定价: 68.00

装帧: 平装

开本: 32开

纸张: 胶版纸

页数: 168页

正文语种: 英语

丛书: 新世纪学术创新团队著作丛书

分类: 自然科学

Thisbookwasdividedintotwopartsandtotalninechapterswereincluded.Inthefirstpart,thebotanical
characters,thegeographicaldistribution,andthepharmacologicalstudiesofSchisandrachinensiswere
introducedrespectively.Inthesecondpart,theextractionmethodsandpurificationtechnologiesofactive
compoundsfromSchisandrachinensisweredescribed.Schisandrachinensisactivecompoundswere
includedthevolatilemolecules-essentialoil,thewatersolublemolecules-anthocyanins,thewatersoluble
macromolecules-polysaccharides,thefatsolublemolecules-biphenylcyclooctenelignans,andthefat
solublemolecules-seedoil.Inaddition,theinsolublemacromolecules-lignocelluloseresidueswererecycled
andpyrolyzedforthepreparationofrenewableenergy,suchasbio-gas,bio-pyroligneousacid,bio-oil,and
bio-char.NotonlyrealizedthefulladvantageofthenaturalactiveproductsinSchisandrachinensisfruits,
andalsozeroemissionstotheenvironment,whichcontributetoenvironmentfriendlycomprehensive
utilizationofthemedicinalresources-Schisandrachinensis. Contents
FOREWORDTOTHESERIES
FOREWORD
PREFACE
PARTISCHISANDRACHINENSIS(TURCZ.)BAILLCHAPTER1INTRODUCTIONOFSCHISANDRACHINENSIS(TURCZ.)BAILL 3
1.1BOTANICALCHARACTERSOFSCHISANDRACHINENSIS 3
1.2GEOGRAPHICALDISTRIBUTIONOFSCHISANDRACHINENSIS 5
REFERENCES 6
CHAPTER2PHARMACOLOGICALSTUDIESOFSCHISANDRACHINENSIS(TURCZ.)BAILL 7
2.1EFFECTONTHECENTRALNERVOUSSYSTEM 7
2.2EFFECTONLIVERPROTECTION 9
2.3ANTIOXIDANTEFFECT 12
2.4ANTI-TUMOREFFECT 13
2.5EFFECTONTHEENDOCRINESYSTEM 15
2.6EFFECTONIMMUNESYSTEM 15
2.7EFFECTONCARDIOVASCULARSYSTEM 16
2.8EFFECTONDIGESTIVESYSTEM 17
REFERENCES 18
CHAPTER3ACTIVECOMPOUNDSOFSCHISANDRACHINENSIS(TURCZ.)BAILL 23
3.1VOLATILEMOLECULES-ESSENTIALOIL 24
3.1.1MainIngredientofSchisandraEssentialOil 24
3.1.2ExtractionMethodsofEssentialOil 25
3.2WATERSOLUBLEMOLECULES-ANTHOCYANIN 28
3.2.1ExtractionMethodsofAnthocyanin 29
3.2.2PurificationMethodsofAnthocyanin 30
3.3WATERSOLUBLEMACROMOLECULES-POLYSACCHARIDES 31
3.3.1ExtractionMethodsofPolysaccharides 31
3.4FATSOLUBLEMOLECULES-BIPHENYLCYCLOOCTENELIGNANS 32
3.4.1MainChemicalCompositionofLignans 32
3.4.2ExtractionMethodsofLignans 33
3.4.3PurificationMethodsoflignans 33
3.5FATSOLUBLEMOLECULES-SEEDOIL 34
3.5.1MainChemicalCompositionofSeedOil 34
3.5.2ExtractionMethodsofSeedOil 34
3.5.3EsterificationMethodsofSeedOil 35
3.6INSOLUBLEMACROMOLECULES-LIGNOCELLULOSERESIDUES 36
REFERENCES 37PARTIIEXTRACTIONSPECIFICEXAMPLESOFACTIVECOMPOUNDSFROMSCHISANDRACHINENSIS(TURCZ.)BAILLCHAPTER4EXTRACTIONOFVOLATILEMOLECULES-ESSENTIALOIL 43
4.1INTRODUCTION 43
4.2MATERIALANDMETHODS 44
4.2.1Material 44
4.2.2Methods 44
4.3RESULTSANDDISCUSSIONS 49
4.3.1SingleFactorofSFME 49
4.3.2OptimalConditionsbyCCD 50
4.3.3AntioxidantActivityTests 52
4.3.4ChemicalCompositionofEssentialOilsbyDifferentExtractionMethod 54
4.3.5Physicalconstantsevaluation 55
4.3.6GeneralMorphologyChangesAfterExtraction 56
4.3.7TGAoftheMaterialAfterExtraction 56
4.3.8Cost,Energy,andEnvironmentImpact 57
4.4CONCLUSIONS 58
REFERENCES 58
CHAPTER5EXTRACTIONOFWATERSOLUBLEMOLECULES-ANTHOCYANIN 60
5.1INTRODUCTION 60
5.2MATERIALANDMETHODS 61
5.2.1Material 61
5.2.2Methods 62
5.3RESULTSANDDISCUSSION 66
5.3.1ExtractionpH 66
5.3.2OptimalConditionsbyBBD 67
5.3.3AdsorptionandDesorption 69
5.3.4ContentandColourStabilityofS.chinensisFruitAnthocyanin 73
5.4CONCLUSIONS 77
REFERENCES 78
CHAPTER6EXTRACTIONOFWATERSOLUBLEMACROMOLECULES-POLYSACCHARIDES 81
6.1INTRODUCTION 81
6.2MATERIALANDMETHODS 82
6.2.1Material 82
6.2.2Methods 83
6.3RESULTSANDDISCUSSION 85
6.3.1StandardCurves 85
6.3.2FactorsofUAEandMAE 86
6.3.3AlternantDigestionbyUAEandMAE 88
6.3.4ComparisonwithDifferentExtractionMethods 90
6.3.5SeparationandPurificationofCrudPolysaccharides 91
6.3.6HydroxylRadical-ScavengingActivityofPolysaccharides 92
6.3.7InVitroActivityofPolysaccharides 94
6.4CONCLUSIONS 95
ConcentsixREFERENCES 95
CHAPTER7EXTRACTIONOFFATSOLUBLEMOLECULES-BIPHENYLCYCLOOCTENELIGNANS 98
7.1INTRODUCTION 98
7.2MATERIALANDMETHODS 101
7.2.1Material 101
7.2.2Methods 103
7.3RESULTSANDDISCUSSION 111
7.3.1HPLCAnalysis 111
7.3.2LC-ESI-MSAnalysis 112
7.3.3Ultrasonic-assistedextraction 112
7.3.4Ultrasonic-AssistedExtractionwithIL 119
7.3.5Microwave-AssistedExtractionwithIL 127
7.3.6StaticIon-ExchangeResinHydrolysisTests 136
7.3.7StaticMacroporousResinAdsorptionandDesorptionTests 138
7.3.8DynamicIon-ExchangeResinHydrolysisCombinedwithMacroporousResinAdsorptionand
DesorptionTests 141
7.3.9HydrolysisMechanismsandHydrolysisEfficiencyofIonExchangeResin 143
7.3.10ReuseofResinsinContinuousProcesses 144
7.3.11DynamicIonic-LiquidHydrolysisCombinedwithMacroporousResinAdsorptionand
DesorptionTests 144
7.4CONCLUSIONS 147
REFERENCES 149
CHAPTER8EXTRACTIONOFFATSOLUBLEMOLECULES-SEEDOIL 153
8.1INTRODUCTION 153
8.2MATERIALANDMETHODS 156
8.2.1Material 156
8.2.2Methods 157
8.3RESULTSANDDISCUSSION 160
8.3.1ExtractionandPropertiesofCrudeSeedOil 160
8.3.2TranseasterificationwithH2SO4asCatalyst 161
8.3.3TranseasterificationwithIon-ExchangeResinasCatalyst 162
8.3.4TranseasterificationwithIonicLiquidasCatalyst 163
8.3.5PropertiesofBiodieselPreparedbyDifferentMethods 164
8.3.6TGAnalysisofCrudeSeedOilandBiodiesel 164
8.3.7FT-IRAnalysisofCrudeSeedOilandBiodiesel 166
8.3.8GC-MSAnalysisofCrudeSeedOilandBiodiesel 166
8.4CONCLUSIONS 167
REFERENCES 167
CHAPTER9PYROLYSISOFINSOLUBLEMACROMOLECULES-LIGNOCELLULOSERESIDUES 170
9.1INTRODUCTION 170
9.2MATERIALANDMETHODS 171
9.2.1Material 171
9.2.2Methods 172
9.3RESULTSANDDISCUSSION 175ChemistryAnalysisandUtilizationofSchisandrachinensis(Turcz.)Baill
9.3.1InfluenceofMoistureContentandMoldingTemperatureontheBriquettingEffect 175
9.3.2PyrolysisCurvesandYieldsofPyrolysisProducts 176
9.3.3SeparationofPAfromBio-Oil 177
9.3.4DeterminationofTotalPhenolicsContent 178
9.3.5DPPHFreeRadicalScavengingActivity 179
9.3.6FerricReducingPower 180
9.3.7ChemicalCompositionofPAExtractsandBio-Oil 181
9.4CONCLUSIONS 184
REFERENCES 185
ABBREVIATIONS 184
内容简介:
Thisbookwasdividedintotwopartsandtotalninechapterswereincluded.Inthefirstpart,thebotanical
characters,thegeographicaldistribution,andthepharmacologicalstudiesofSchisandrachinensiswere
introducedrespectively.Inthesecondpart,theextractionmethodsandpurificationtechnologiesofactive
compoundsfromSchisandrachinensisweredescribed.Schisandrachinensisactivecompoundswere
includedthevolatilemolecules-essentialoil,thewatersolublemolecules-anthocyanins,thewatersoluble
macromolecules-polysaccharides,thefatsolublemolecules-biphenylcyclooctenelignans,andthefat
solublemolecules-seedoil.Inaddition,theinsolublemacromolecules-lignocelluloseresidueswererecycled
andpyrolyzedforthepreparationofrenewableenergy,suchasbio-gas,bio-pyroligneousacid,bio-oil,and
bio-char.NotonlyrealizedthefulladvantageofthenaturalactiveproductsinSchisandrachinensisfruits,
andalsozeroemissionstotheenvironment,whichcontributetoenvironmentfriendlycomprehensive
utilizationofthemedicinalresources-Schisandrachinensis.
目录:
Contents
FOREWORDTOTHESERIES
FOREWORD
PREFACE
PARTISCHISANDRACHINENSIS(TURCZ.)BAILLCHAPTER1INTRODUCTIONOFSCHISANDRACHINENSIS(TURCZ.)BAILL 3
1.1BOTANICALCHARACTERSOFSCHISANDRACHINENSIS 3
1.2GEOGRAPHICALDISTRIBUTIONOFSCHISANDRACHINENSIS 5
REFERENCES 6
CHAPTER2PHARMACOLOGICALSTUDIESOFSCHISANDRACHINENSIS(TURCZ.)BAILL 7
2.1EFFECTONTHECENTRALNERVOUSSYSTEM 7
2.2EFFECTONLIVERPROTECTION 9
2.3ANTIOXIDANTEFFECT 12
2.4ANTI-TUMOREFFECT 13
2.5EFFECTONTHEENDOCRINESYSTEM 15
2.6EFFECTONIMMUNESYSTEM 15
2.7EFFECTONCARDIOVASCULARSYSTEM 16
2.8EFFECTONDIGESTIVESYSTEM 17
REFERENCES 18
CHAPTER3ACTIVECOMPOUNDSOFSCHISANDRACHINENSIS(TURCZ.)BAILL 23
3.1VOLATILEMOLECULES-ESSENTIALOIL 24
3.1.1MainIngredientofSchisandraEssentialOil 24
3.1.2ExtractionMethodsofEssentialOil 25
3.2WATERSOLUBLEMOLECULES-ANTHOCYANIN 28
3.2.1ExtractionMethodsofAnthocyanin 29
3.2.2PurificationMethodsofAnthocyanin 30
3.3WATERSOLUBLEMACROMOLECULES-POLYSACCHARIDES 31
3.3.1ExtractionMethodsofPolysaccharides 31
3.4FATSOLUBLEMOLECULES-BIPHENYLCYCLOOCTENELIGNANS 32
3.4.1MainChemicalCompositionofLignans 32
3.4.2ExtractionMethodsofLignans 33
3.4.3PurificationMethodsoflignans 33
3.5FATSOLUBLEMOLECULES-SEEDOIL 34
3.5.1MainChemicalCompositionofSeedOil 34
3.5.2ExtractionMethodsofSeedOil 34
3.5.3EsterificationMethodsofSeedOil 35
3.6INSOLUBLEMACROMOLECULES-LIGNOCELLULOSERESIDUES 36
REFERENCES 37PARTIIEXTRACTIONSPECIFICEXAMPLESOFACTIVECOMPOUNDSFROMSCHISANDRACHINENSIS(TURCZ.)BAILLCHAPTER4EXTRACTIONOFVOLATILEMOLECULES-ESSENTIALOIL 43
4.1INTRODUCTION 43
4.2MATERIALANDMETHODS 44
4.2.1Material 44
4.2.2Methods 44
4.3RESULTSANDDISCUSSIONS 49
4.3.1SingleFactorofSFME 49
4.3.2OptimalConditionsbyCCD 50
4.3.3AntioxidantActivityTests 52
4.3.4ChemicalCompositionofEssentialOilsbyDifferentExtractionMethod 54
4.3.5Physicalconstantsevaluation 55
4.3.6GeneralMorphologyChangesAfterExtraction 56
4.3.7TGAoftheMaterialAfterExtraction 56
4.3.8Cost,Energy,andEnvironmentImpact 57
4.4CONCLUSIONS 58
REFERENCES 58
CHAPTER5EXTRACTIONOFWATERSOLUBLEMOLECULES-ANTHOCYANIN 60
5.1INTRODUCTION 60
5.2MATERIALANDMETHODS 61
5.2.1Material 61
5.2.2Methods 62
5.3RESULTSANDDISCUSSION 66
5.3.1ExtractionpH 66
5.3.2OptimalConditionsbyBBD 67
5.3.3AdsorptionandDesorption 69
5.3.4ContentandColourStabilityofS.chinensisFruitAnthocyanin 73
5.4CONCLUSIONS 77
REFERENCES 78
CHAPTER6EXTRACTIONOFWATERSOLUBLEMACROMOLECULES-POLYSACCHARIDES 81
6.1INTRODUCTION 81
6.2MATERIALANDMETHODS 82
6.2.1Material 82
6.2.2Methods 83
6.3RESULTSANDDISCUSSION 85
6.3.1StandardCurves 85
6.3.2FactorsofUAEandMAE 86
6.3.3AlternantDigestionbyUAEandMAE 88
6.3.4ComparisonwithDifferentExtractionMethods 90
6.3.5SeparationandPurificationofCrudPolysaccharides 91
6.3.6HydroxylRadical-ScavengingActivityofPolysaccharides 92
6.3.7InVitroActivityofPolysaccharides 94
6.4CONCLUSIONS 95
ConcentsixREFERENCES 95
CHAPTER7EXTRACTIONOFFATSOLUBLEMOLECULES-BIPHENYLCYCLOOCTENELIGNANS 98
7.1INTRODUCTION 98
7.2MATERIALANDMETHODS 101
7.2.1Material 101
7.2.2Methods 103
7.3RESULTSANDDISCUSSION 111
7.3.1HPLCAnalysis 111
7.3.2LC-ESI-MSAnalysis 112
7.3.3Ultrasonic-assistedextraction 112
7.3.4Ultrasonic-AssistedExtractionwithIL 119
7.3.5Microwave-AssistedExtractionwithIL 127
7.3.6StaticIon-ExchangeResinHydrolysisTests 136
7.3.7StaticMacroporousResinAdsorptionandDesorptionTests 138
7.3.8DynamicIon-ExchangeResinHydrolysisCombinedwithMacroporousResinAdsorptionand
DesorptionTests 141
7.3.9HydrolysisMechanismsandHydrolysisEfficiencyofIonExchangeResin 143
7.3.10ReuseofResinsinContinuousProcesses 144
7.3.11DynamicIonic-LiquidHydrolysisCombinedwithMacroporousResinAdsorptionand
DesorptionTests 144
7.4CONCLUSIONS 147
REFERENCES 149
CHAPTER8EXTRACTIONOFFATSOLUBLEMOLECULES-SEEDOIL 153
8.1INTRODUCTION 153
8.2MATERIALANDMETHODS 156
8.2.1Material 156
8.2.2Methods 157
8.3RESULTSANDDISCUSSION 160
8.3.1ExtractionandPropertiesofCrudeSeedOil 160
8.3.2TranseasterificationwithH2SO4asCatalyst 161
8.3.3TranseasterificationwithIon-ExchangeResinasCatalyst 162
8.3.4TranseasterificationwithIonicLiquidasCatalyst 163
8.3.5PropertiesofBiodieselPreparedbyDifferentMethods 164
8.3.6TGAnalysisofCrudeSeedOilandBiodiesel 164
8.3.7FT-IRAnalysisofCrudeSeedOilandBiodiesel 166
8.3.8GC-MSAnalysisofCrudeSeedOilandBiodiesel 166
8.4CONCLUSIONS 167
REFERENCES 167
CHAPTER9PYROLYSISOFINSOLUBLEMACROMOLECULES-LIGNOCELLULOSERESIDUES 170
9.1INTRODUCTION 170
9.2MATERIALANDMETHODS 171
9.2.1Material 171
9.2.2Methods 172
9.3RESULTSANDDISCUSSION 175ChemistryAnalysisandUtilizationofSchisandrachinensis(Turcz.)Baill
9.3.1InfluenceofMoistureContentandMoldingTemperatureontheBriquettingEffect 175
9.3.2PyrolysisCurvesandYieldsofPyrolysisProducts 176
9.3.3SeparationofPAfromBio-Oil 177
9.3.4DeterminationofTotalPhenolicsContent 178
9.3.5DPPHFreeRadicalScavengingActivity 179
9.3.6FerricReducingPower 180
9.3.7ChemicalCompositionofPAExtractsandBio-Oil 181
9.4CONCLUSIONS 184
REFERENCES 185
ABBREVIATIONS 184

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北五味子化学成分分析及利用（英文版）

内容简介:

目录: